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Center for Emerging Energy Sciences

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Projects  -  Advanced Materials Fabrication & Diagnostics:

AI Feature Identification: Platinum islands & volcanoes

 

 

Tritium extraction

Tritium extraction can usually be achieved with ~60% efficiency before measuring the activity using a 2009 Quantulus GCT 6220 Scintillator, which has a detection limit of about one femtomole.

QuantulusA     Quantulus_Measurements

 

 

Absorbed atmospheric 4He in various technical materials

Total helium amount outgassed and release temperature of out-gassing from different materials.:

Sample Weight / Size Baking Temerature (°C) 4He Outgassing (picomoles) 4He Outgassing (picomoles / gram) Outgassing Temperature (°C)
Blank Palladium plate --- 600 2.7 --- ---
PTFE 1.25 g 450 281 224.8 ---
Large PTFE Tube 1.009 g 600 50 49.55 above melting temperature of PTFE  
Small PTFE Tube 1.006 g 500 87 86.48 above melting temperature of PTFE  
AWG PTFE Tube 1.006 g 500 48 47.71 above melting temperature of PTFE
MACOR as delivered 13 g 600 280 21.54 600
MACOR Prebaked, 2 days in atmosphere 13 g 600 110 8.46 ---
MACOR Soaked in 4He for 8 hours (25 °C) 13 g Room Temperature 5400 415.38 Room Temperature
MACOR Soaked in 4He for 8 hours (600 °C) 13 g 600 3800 292.31 ---
CF Cell Diffusion Test --- Room Temperature 500 --- Room Temperature
4He-Soaked CF Cell 2 --- Room Temperature 290000 --- Room Temperature
(4) 3" Teflon Stripes, McMaster 7.061 g 600 7100 1005.5 380
(4) Nylon Nuts 0.191 g 400 1.6 8.38 No sign of outgassing
Nylon Screws 0.184 g 400 3.6 19.57 No sign of outgassing
PTFE TWTT-22C 0.66 g 550 9.9 15 360
PTFE Plate Washer 3.857 g 550 19 4.93 360
Nylon Nuts 0.807 g 400 0.8 0.99 No sign of outgassing
Nylon Screws 0.921 g 400 0.44 0.48 No sign of outgassing
Pd #2 wire 0.009" Diameter 12" 9.15 g   21.3 202.9 evaporation
Pd #1 wire 0.009" Diameter 12" 0.15 g   3.83 25.5 evaporation
SS304 Capillary 0.32 g   19.4 60.6 evaporation

·       PTFE melting temperature: 327 °C

·       Nylon melting temperature: 220 °C; decomposition temperature: 307 °C

 

 

 

Deuterium and Protium Purification System

We have developed a method that eliminates the 4He isotopes from the as-delivered stock supply of protium or deuterium gas.   Our FT-ICR MS techniques described above are used to determine the low ambient level of 4He in this supply gas.  In all cases encountered to date, the ambient 4He concentrations in hydrogen supply gasses have been lowered to undetectable levels (< 0.001 ppm). We also purge the environments that surround our cells and instruments to < 0.005 ppm of 4He, to prevent any accidental mis-interpretation of ambient 4He for produced 4He in our experiments. We also check for any air invasion isotopes (20Ne or 40Ar) in every aliquot during mass spectrometry.

Purifier

Purify_D2

Purify_H2

 

 

 

 

 

Focused Ion Beam

DynaCool

Collaborative Projects Using Dynacool

DynaCool

Zeiss Crossbeam 540 Nanostructure characterization