Center for Emerging Energy Sciences
Projects - Advanced Materials Fabrication & Diagnostics:
AI Feature Identification: Platinum islands & volcanoes
Tritium extraction
Tritium extraction can usually be achieved with ~60% efficiency before measuring the activity using a 2009 Quantulus GCT 6220 Scintillator, which has a detection limit of about one femtomole.
Absorbed atmospheric 4He in various technical materials
Total helium amount outgassed and release temperature of out-gassing from different materials.:
Sample | Weight / Size | Baking Temerature (°C) | 4He Outgassing (picomoles) | 4He Outgassing (picomoles / gram) | Outgassing Temperature (°C) |
Blank Palladium plate | --- | 600 | 2.7 | --- | --- |
PTFE | 1.25 g | 450 | 281 | 224.8 | --- |
Large PTFE Tube | 1.009 g | 600 | 50 | 49.55 | above melting temperature of PTFE |
Small PTFE Tube | 1.006 g | 500 | 87 | 86.48 | above melting temperature of PTFE |
AWG PTFE Tube | 1.006 g | 500 | 48 | 47.71 | above melting temperature of PTFE |
MACOR as delivered | 13 g | 600 | 280 | 21.54 | 600 |
MACOR Prebaked, 2 days in atmosphere | 13 g | 600 | 110 | 8.46 | --- |
MACOR Soaked in 4He for 8 hours (25 °C) | 13 g | Room Temperature | 5400 | 415.38 | Room Temperature |
MACOR Soaked in 4He for 8 hours (600 °C) | 13 g | 600 | 3800 | 292.31 | --- |
CF Cell Diffusion Test | --- | Room Temperature | 500 | --- | Room Temperature |
4He-Soaked CF Cell 2 | --- | Room Temperature | 290000 | --- | Room Temperature |
(4) 3" Teflon Stripes, McMaster | 7.061 g | 600 | 7100 | 1005.5 | 380 |
(4) Nylon Nuts | 0.191 g | 400 | 1.6 | 8.38 | No sign of outgassing |
Nylon Screws | 0.184 g | 400 | 3.6 | 19.57 | No sign of outgassing |
PTFE TWTT-22C | 0.66 g | 550 | 9.9 | 15 | 360 |
PTFE Plate Washer | 3.857 g | 550 | 19 | 4.93 | 360 |
Nylon Nuts | 0.807 g | 400 | 0.8 | 0.99 | No sign of outgassing |
Nylon Screws | 0.921 g | 400 | 0.44 | 0.48 | No sign of outgassing |
Pd #2 wire 0.009" Diameter 12" | 9.15 g | 21.3 | 202.9 | evaporation | |
Pd #1 wire 0.009" Diameter 12" | 0.15 g | 3.83 | 25.5 | evaporation | |
SS304 Capillary | 0.32 g | 19.4 | 60.6 | evaporation |
· PTFE melting temperature: 327 °C
· Nylon melting temperature: 220 °C; decomposition temperature: 307 °C
Deuterium and Protium Purification System
We have developed a method that eliminates the 4He isotopes from the as-delivered stock supply of protium or deuterium gas. Our FT-ICR MS techniques described above are used to determine the low ambient level of 4He in this supply gas. In all cases encountered to date, the ambient 4He concentrations in hydrogen supply gasses have been lowered to undetectable levels (< 0.001 ppm). We also purge the environments that surround our cells and instruments to < 0.005 ppm of 4He, to prevent any accidental mis-interpretation of ambient 4He for produced 4He in our experiments. We also check for any air invasion isotopes (20Ne or 40Ar) in every aliquot during mass spectrometry.
Focused Ion Beam
DynaCool
Collaborative Projects Using Dynacool
Zeiss Crossbeam 540 Nanostructure characterization
Department of Physics and Astronomy
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Address
Texas Tech University, Physics & Astronomy Department, Box 41051, Lubbock, TX 79409-1051 -
Phone
806.742.3767 | Fax: 806.742.1182 -
Email
physics.astronomy.webmasters@ttu.edu | physics.academic.advising@ttu.edu